Adsorption hplc sampler vials

TruView autosampler vials are rigorously tested for dimensional characteristics, cleanliness with mass spectrometry, and adsorption using a variety of techniques including UPLC-UV and UPLC-MS and impact on analyte pH. Unlike today’s standard vials, TruView Vials are the only vials tested and certified for low analyte adsorption at 1 ng/mL and

May 10, 2016 · May 10 2016. Supelco’s Low Adsorption (LA) vials are manufactured using a process that decreases the number of hydroxyl groups on the vial's glass surface, significantly reducing surface activity while improving analytical quantitation and minimising pH shifts in the sample. This same process also removes unwanted surface metals such as

May 1, 2015 · HPLC autosampler vials (2 mL, dimensions 12 × 32 mm, borosilicate glass, product no. C4010-1), screw caps for HPLC autosampler vials (open top cap, polypropylene, product no. C4010-1A), and septa for screw caps (diameter 10 mm, PTFE/silicone, product no. C4010-40) were purchased from National Scientific (Rockwood, TN).

Innovative and carefully designed Thermo Scientific autosamplers and sampler extension module ensure reliable, precise and accurate injection for nanoliter to milliliter sample volumes. They support a wide range of formats and sample throughputs. Choose from rapid separation, nano, capillary, micro, standard, semi-preparative and more.

4608 Well Plates, 840 × 0.5 mL or 0.7 mL Vials, 648 × 2 mL Sample Vials, 240 × 10 mL or 20 mL Vials: Injection Mode: 8 Fully Customizable Method-Specific Injection Mode Presets: Injection Speed: Selectable from 0.1 μL/s to 2000 μL/s: Injection Volume: Description: TriPlus RSH SMART configured for liquid injection on regular X-axis length.

Fisherbrand™ spring vial inserts are compatible with 8 mm HPLC and GC autosampler vials. 8 DWK Life Sciences MicroLiter Limited Volume Inserts for 9mm and 11mm Autosampler Vials, Silanized MicroLiter limited volume inserts are made from Type 1 borosilicate glass or polypropylene and meet strict tolerances.

The Concept Behind TORAST-H Vials. The composition of the raw material used in the manufacture of vials varies depending on the type of glass, but in general 70-75% is SiO 2, and the rest consists of metal (M) oxides. Metal oxides are added, for example, to improve the moldability of the glass by lowering its melting point.

Acidic compounds and neutral compounds mainly adsorb to glass and PP containers by hydrophobic adsorption. Therefore, an organic solvent (methanol, acetonitrile, etc.) or non-ionic surfactant is added to the sample solution to reduce adsorption. Although dependent on the logP of the target compounds, adding 10 to 50 % organic solvent or around

Certified LCMS Certified Closure Type Screw Neck Cap Color Blue Dimensions 12 x 32 mm Format Total Recovery Vial. Material Clear Glass Seal Material preslit PTFE/Silicone Volume Capacity 1 mL Type Autosampler vial Includes Vial, Cap, & Septum. SKU: 186002639. Polypropylene 12 x 32 mm Screw Neck Vial, with Cap and Preslit PTFE/Silicone Septum

When this mechanism is translated to the phenomenon of sample adsorption to containers, the stationary phase becomes the container material, the mobile phase becomes the sample solution being prepared, and the retention behavior of materials adsorbed onto containers is the adsorption strength. Fig. 1 Mechanism of Adsorption to Vials and Methods for Inhibiting Adsorption.

Low Adsorption HPLC Columns Based on MaxPeak High Performance Surfaces 3 HITE PAPER Figure 3. Benefits of MaxPeak HPS Technology for LC-MS analyses. (A) MS chromatogram of tryptic peptide 37 from NISTmAb using a gradient separation with mobile phases containing 0.1% (v/v) formic acid with ACQUITY UPLC CSH™ C 18,

Adsorption to glass vials is known to be mainly by ionic adsorption to silanol groups at the glass surface, and adsorption to polymer vials such as PP vials is known to be mainly by hydrophobic adsorption to the polymer surface. Fig. 4 shows a comparison between different types of vials using a tryptic digest of myoglobin as the sample.

We provide a complete range of high-quality products for accurate, brilliant results in a variety of analytical applications, including HPLC, GC, Karl Fischer titration, elemental trace analysis, classical analysis, air monitoring, food and beverage analysis, and proficiency testing. We also supply a complete range of safety equipment.

Sep 5, 2014 · Abstract. In the drug-discovery setting, the development of new peptide and protein-based biopharmaceuticals attracts increased attention from the pharmaceutical industry and consequently demands the development of high-throughput LC-MS methods. Regulatory guidelines require bioanalytical methods to be validated not only in terms of linearity, sensitivity, accuracy, precision, selectivity and stability, but also in terms of carryover.

GC: Vials are most applicable with GC methods with longer run-times. The glass vials are more compatible with the strong organic solvents used to solubilize liquid samples. HPLC: When processing samples in batches of less than 50 use vials as there is little advantage using a 96-well plate as the plate capacity would not be fully utilized.